{"id":9794,"date":"2026-08-09T14:37:49","date_gmt":"2026-08-09T06:37:49","guid":{"rendered":"\/jase\/?post_type=tkuisotope&#038;p=9794"},"modified":"2026-08-09T16:00:47","modified_gmt":"2026-08-09T08:00:47","slug":"jase-202611-34-027","status":"publish","type":"tkuisotope","link":"\/jase\/?tkuisotope=jase-202611-34-027","title":{"rendered":"Study on the pyrolysis characteristics and stepwise heating release behavior of aroma substances from different types of tobacco leaves"},"content":{"rendered":"\n<div class=\"wp-block-tkuwpbs5-bs5-row row article-info\">\n<div class=\"wp-block-tkuwpbs5-bs5-column col-md-3 align-self-start\">\n<p><i class=\"fa fa-folder\" aria-hidden=\"true\"><\/i>&nbsp;<a href=\"\/jase\/?page_id=807\" data-type=\"page\" data-id=\"807\">2026<\/a><\/p>\n<\/div>\n\n\n\n<div class=\"wp-block-tkuwpbs5-bs5-column col-md-3 align-self-start\">\n<p><i class=\"fa fa-folder-open\" aria-hidden=\"true\"><\/i>&nbsp;<a href=\"\/jase\/?page_id=9439\" data-type=\"page\" data-id=\"9439\">Volume 34<\/a><\/p>\n<\/div>\n\n\n\n<div class=\"wp-block-tkuwpbs5-bs5-column col-md-6 align-self-start\">\n<div class=\"wp-block-tkuwpbs5-bs5-div dv_publish\" data-aos=\"normal\"><div class=\"wp-block-post-date\"><time datetime=\"2026-08-09T14:37:49+08:00\">2026-08-09<\/time><\/div><\/div>\n<\/div>\n<\/div>\n\n\n\n<div class=\"wp-block-tkuwpbs5-bs5-row row\">\n<div class=\"wp-block-tkuwpbs5-bs5-column col-md-5 align-self-start\">\n<div class=\"wp-block-tkuwpbs5-bs5-div au-ol\" data-aos=\"normal\">\n<p>Miao Liang<sup>1<\/sup>, Wenqi Li<sup>1<\/sup>, Jiao Li<sup>2<\/sup>, Huijuan Dai<sup>2<\/sup>, Yanbin Zhou<sup>2<\/sup><a href=\"mailto:hbzyzyb@163.com\"><i class=\"fa fa-envelope\"><\/i><\/a>, Mengshu Ran<sup>1<\/sup>, Guanyun Liu<sup>1<\/sup>, and Junsong Zhang<sup>1<\/sup><a href=\"mailto:13283712413@163.com\"><i class=\"fa fa-envelope\"><\/i><\/a><\/p>\n\n\n\n<p style=\"font-size:14px\"><sup>1<\/sup>College of Tobacco Science and Engineering, Zhengzhou University of Light Industry, Zhengzhou, 450001, P. R. China<\/p>\n\n\n\n<p style=\"font-size:14px\"><sup>2<\/sup>China Tobacco Hebei Industrial Co., Ltd, Shijiazhuang, 050051, P. R. China<\/p>\n<\/div>\n\n\n\n<div class=\"wp-block-tkuwpbs5-bs5-div\" style=\"margin-top:var(--wp--preset--spacing--40)\" data-aos=\"normal\">\n<p>Received: May 08, 2026<br>Accepted: July 13, 2026<br>Publication Date:&nbsp;August 09, 2026<\/p>\n<\/div>\n<\/div>\n\n\n\n<div class=\"wp-block-tkuwpbs5-bs5-column col-md-7 align-self-start clk=\u5716\u7247\"><img decoding=\"async\" src=\"\/jase\/wp-content\/uploads\/2026\/08\/34_027.jpg\" class=\"img-fluid img-fluid mx-auto d-block\" alt=\"\u4e0a\u50b3\u5716\u7247\">\n\n\n<p class=\"has-text-align-center\">Schematic&nbsp;diagram&nbsp;of&nbsp;programmed&nbsp;heating&nbsp;platform&nbsp;and&nbsp;gas&nbsp;collection system&nbsp;<\/p>\n<\/div>\n<\/div>\n\n\n\n<p class=\"has-small-font-size\"><i class=\"fab fa-creative-commons\"><\/i>&nbsp;<strong>Copyright&nbsp;<\/strong>The Author(s). This is an open access article distributed under the terms of the&nbsp;<a rel=\"noreferrer noopener\" href=\"https:\/\/creativecommons.org\/licenses\/by\/4.0\/\" target=\"_blank\">Creative Commons Attribution&nbsp;License (CC BY 4.0)<\/a>, which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are cited.<\/p>\n\n\n\n<p>Download Citation:\u00a0 <a href=\"\/jase\/wp-content\/uploads\/2026\/08\/V34.0027.txt\" data-type=\"attachment\" data-id=\"9816\" target=\"_blank\" rel=\"noreferrer noopener\">BibTeX <\/a>| <a rel=\"noreferrer noopener\" href=\"http:\/\/dx.doi.org\/10.6180\/jase.202611_34.027\" target=\"_blank\">http:\/\/dx.doi.org\/10.6180\/jase.202611_34.027<\/a>\u00a0\u00a0<\/p>\n\n\n\n<p class=\"btn btn-primary article-btn\"><a href=\"\/jase\/wp-content\/uploads\/2026\/08\/027_2026_0988_V34.pdf\" data-type=\"attachment\" data-id=\"9780\" target=\"_blank\" rel=\"noreferrer noopener\">Download PDF<\/a><\/p>\n\n\n\n<div style=\"height:24px\" aria-hidden=\"true\" class=\"wp-block-spacer\"><\/div>\n\n\n\n<p>To investigate the differences in thermogravimetric characteristics and heat release behavior of various tobacco leaves, flue-cured, oriental, and Cuibi No. 1 tobaccos were analyzed using thermogravimetric analysis coupled with a programmed heating platform and gas collection system. Partial least squares discriminant analysis (OPLS-DA) was employed to identify key differential substances across heating stages. The thermal weight-loss<br>process for all samples comprised four stages, with characteristic parameters varying significantly among tobacco types. Oriental tobacco exhibited a higher weight-loss rate at stage II, while Cuibi No. 1 demonstrated a superior comprehensive pyrolysis index of 3.36 \u00d7 10<sup>\u22124<\/sup> (%\/min \u00b7 <sup>\u25e6<\/sup>C<sup>2<\/sup>). Kinetic analysis revealed that the F1.5-order chemical reaction model adequately described the decomposition processes. Activation energy at stage II ranged from 54.30 to 89.20 kJ\/mol, with flue-cured tobacco showing significantly higher activation energy at stage III than the other two types. Stage II was identified as the primary phase for aroma product formation, where the total release amount followed the order: flue-cured tobacco (15,278.56 \u00b5g\/g) &gt; oriental tobacco (14,974.00 \u00b5g\/g) &gt; Cuibi No. 1 (13,190.34 \u00b5g\/g), with aroma components accounting for over 84% of the total aroma compounds for each variety. OPLS-DA identified 20, 10, and 5 key differential substances for stages II, III and IV, respectively. These findings provide data support for understanding quality characteristics of tobacco materials and may offer guidance for product formulation design.<\/p>\n\n\n\n<p><em>Keywords:&nbsp;thermogravimetric characteristics; stepwise heating; tobacco leaf type; heat released products; partial least squares discriminant analysis<\/em><\/p>\n\n\n\n<div style=\"height:2rem\" aria-hidden=\"true\" class=\"wp-block-spacer\"><\/div>\n\n\n\n<div class=\"wp-block-tkuwpbs5-bs5-div ref_ol\" data-aos=\"normal\">\n<ol>\n<li>[1] A. Gomez-Siurana, A. Marcilla, M. Beltran, D. Berenguer, I. Martinez-Castellanos, and S. Menargues, (2013) \u201cTGA\/FTIR study of tobacco and glycerol-tobacco mixtures\u201d THERMOCHIMICA ACTA 573: 146\u2013157. DOI: 10.1016\/j.tca.2013.09.007.<\/li>\n<li>[2] W. Wu, Y. Mei, L. Zhang, R. Liu, and J. Cai, (2015) \u201cKinetics and reaction chemistry of pyrolysis and combustion of tobacco waste\u201d FUEL 156: 71\u201380. DOI: 10.1016\/j.fuel.2015.04.016.<\/li>\n<li>[3] M. Liang, T. Yang, G. Zhang, K. Zhang, L. Wang, R. Li, Y. He, J. Wang, and J. Zhang, (2023) \u201cEffects of hydrochloric acid washing on the structure and pyrolysis characteristics of tobacco stalk\u201d BIOMASS CONVERSION AND BIOREFINERY 13(8): 6817\u20136830. DOI: 10.1007\/s13399-021-01616-5.<\/li>\n<li>[4] M. Liang, Y. Wang, S. Dai, L. Hong, R. Li, Z. Xu, J. Su, and J. Zhang, (2025) \u201cEffect of glycerol addition and heating rate on the thermal release behavior of cigar tobacco\u201d BIOMASS CONVERSION AND BIOREFINERY 15(4, SI): 6071\u20136086. DOI: 10.1007\/s13399-024-05484-7.<\/li>\n<li>[5] T. Adam, T. Ferge, S. Mitschke, T. Streibel, R. Baker, and R. Zimmermann, (2005) \u201cDiscrimination of three tobacco types (Burley, Virginia and Oriental) by pyrolysis single-photon ionisation-time-of-flight mass spectrometry and advanced statistical methods\u201d ANALYTICAL AND BIOANALYTICAL CHEMISTRY 381(2): 487\u2013499. DOI: 10.1007\/s00216-004-2935-0.<\/li>\n<li>[6] Z. Jiabao, W. Yiqun, L. Miao, Z. Xinchao, W. Dongchuan, and Z. Junsong, (2023) \u201cLow temperature pyrolysis characteristics of heated tobacco raw materials and its correlation with sensory quality\u201d JOURNAL OF LIGHT INDUSTRY 38(3): 94\u2013101. DOI: 10.12187 \/ 2023.03.012.<\/li>\n<li>[7] M. Liang, H. Pan, Y. Zhu, H. Zhu, M. Su, Y. Xie, Y. Zheng, X. Jiang, R. Li, and J. Zhang, (2023) \u201cCo-pyrolysis behavior of polylactic acid and biomass from heated tobacco products\u201d BIOMASS CONVERSION AND BIOREFINERY: DOI: 10.1007 \/ s13399-023-04575-1.<\/li>\n<li>[8] X. Jiang, J. Wu, L. Zhao, J. Wang, W. Xiao, Z. Chen, J. Jiang, M. Liang, J. Wang, and J. Zhang, (2025) \u201cStudy on the Pyrolysis Behaviour of Different Types of Tobacco and Their Pyrolytic Aroma Components Distribution Under Stepwise Heating Conditions\u201d FLAVOUR AND FRAGRANCE JOURNAL 40(3): 512\u2013527. DOI: 10.1002\/ffj.3857.<\/li>\n<li>[9] M. Liang, J. Zhang, B. Li, Q. Fu, Y. Hu, Z. Ren, R. Li, C. Cui, and J. Zhang, (2025) \u201cComparative Study On The Pyrolysis Characteristics And Gaseous Release Behavior Of Different Reconstituted Tobacco Cut Stem In Processing\u201d JOURNAL OF APPLIED SCIENCE AND ENGINEERING 29(2): 359\u2013368. DOI: 10.6180\/jase.202602_29(2).0011.<\/li>\n<li>[10] K. Aurreethum, V. Sricharoenchaikul, P. R. Kaewpengkrow, and M. Khemkhao, (2026) \u201cEnhancing Pyrolysis Oil From Landfill Waste Plastic With Industrial Waste Catalyst\u201d JOURNAL OF APPLIED SCIENCE AND ENGINEERING 29(4): 1003\u20131019. DOI: 10.6180\/jase.202603_29(4).0023.<\/li>\n<li>[11] B. Saha, S. Koley, M. Khwairakpam, and A. S. Kalamdhad, (2022) \u201cComparative study between mono-digestion and co-digestion of terrestrial weed (Parthenium hysterophorus)\u201d CLEANER ENGINEERING AND TECHNOLOGY 11: DOI: 10.1016\/j.clet.2022.100560.<\/li>\n<li>[12] B. Saha, A. S. Kalamdhad, and M. Khwairakpam, (2021) \u201cEfficiency of electrohydrolysis pretreatment on terrestrial weed (Parthenium hysterophorus) to cut down the hydrolysis stage during the anaerobic digestion process and continuous reactor study\u201d ENERGY REPORTS 7: 3547\u20133555. DOI: 10.1016\/j.egyr.2021.06.023.<\/li>\n<\/ol>\n<\/div>\n\n\n\n<p><\/p>\n","protected":false},"author":3,"template":"wp-custom-template-detail-4-aricles","meta":{"_uag_custom_page_level_css":""},"categories":[12,1682,6],"tags":[1709],"acf":[],"uagb_featured_image_src":[],"uagb_author_info":{"display_name":"\u6797\u923a\u6db5","author_link":"\/jase\/?author=3"},"uagb_comment_info":0,"uagb_excerpt":"&nbsp;Copyright&nbsp;The Author(s). This is an open access article distributed under the terms of the&nbsp;Creative Commons Attribution&nbsp;License (CC BY 4.0), which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are cited. Download Citation:\u00a0 BibTeX | http:\/\/dx.doi.org\/10.6180\/jase.202611_34.027\u00a0\u00a0 Download PDF To investigate the differences in thermogravimetric characteristics and heat release behavior&hellip;","_links":{"self":[{"href":"\/jase\/index.php?rest_route=\/wp\/v2\/tkuisotope\/9794"}],"collection":[{"href":"\/jase\/index.php?rest_route=\/wp\/v2\/tkuisotope"}],"about":[{"href":"\/jase\/index.php?rest_route=\/wp\/v2\/types\/tkuisotope"}],"author":[{"embeddable":true,"href":"\/jase\/index.php?rest_route=\/wp\/v2\/users\/3"}],"wp:attachment":[{"href":"\/jase\/index.php?rest_route=%2Fwp%2Fv2%2Fmedia&parent=9794"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"\/jase\/index.php?rest_route=%2Fwp%2Fv2%2Fcategories&post=9794"},{"taxonomy":"post_tag","embeddable":true,"href":"\/jase\/index.php?rest_route=%2Fwp%2Fv2%2Ftags&post=9794"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}